In this study, hydroxyapatite (HAp) coatings were deposited on Ti plates by the high-velocity suspension flame spraying (HVSFS) technique. The process characteristic, the microstructure and phase composi- tion of the coatings are significantly influenced by the solvent and by the design of the combustion chamber (CC) of the HVSFS torch. Water-based suspensions always lead to fairly low surface tem- peratures ( 350 °C), deposition efficiencies <40%, and produce coatings with low amount of crystalline HAp, which tend to dissolve very rapidly in simulated body fluid (SBF) solutions. DEG-based suspen- sions, when sprayed with properly-designed CCs, produce deposition efficiencies of 45-55% and high surface temperatures (550-600 °C). In these coatings, the degree of crystallinity increases from the bottom layer to the top layer, probably because the increasingly large surface temperature can eventually favour re-crystallisation of individual lamellae during cooling. These coatings are much more stable in SBF solutions.

High Velocity Suspension Flame Sprayed (HVSFS) Hydroxyapatite Coatings for Biomedical Applications / N., Stiegler; Bellucci, Devis; Bolelli, Giovanni; Cannillo, Valeria; R., Gadow; A., Killinger; Lusvarghi, Luca; Sola, Antonella. - In: JOURNAL OF THERMAL SPRAY TECHNOLOGY. - ISSN 1059-9630. - STAMPA. - 21:(2012), pp. 275-287. [10.1007/s11666-011-9724-z]

High Velocity Suspension Flame Sprayed (HVSFS) Hydroxyapatite Coatings for Biomedical Applications

BELLUCCI, Devis;BOLELLI, Giovanni;CANNILLO, Valeria;LUSVARGHI, Luca;SOLA, Antonella
2012-01-01

Abstract

In this study, hydroxyapatite (HAp) coatings were deposited on Ti plates by the high-velocity suspension flame spraying (HVSFS) technique. The process characteristic, the microstructure and phase composi- tion of the coatings are significantly influenced by the solvent and by the design of the combustion chamber (CC) of the HVSFS torch. Water-based suspensions always lead to fairly low surface tem- peratures ( 350 °C), deposition efficiencies <40%, and produce coatings with low amount of crystalline HAp, which tend to dissolve very rapidly in simulated body fluid (SBF) solutions. DEG-based suspen- sions, when sprayed with properly-designed CCs, produce deposition efficiencies of 45-55% and high surface temperatures (550-600 °C). In these coatings, the degree of crystallinity increases from the bottom layer to the top layer, probably because the increasingly large surface temperature can eventually favour re-crystallisation of individual lamellae during cooling. These coatings are much more stable in SBF solutions.
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High Velocity Suspension Flame Sprayed (HVSFS) Hydroxyapatite Coatings for Biomedical Applications / N., Stiegler; Bellucci, Devis; Bolelli, Giovanni; Cannillo, Valeria; R., Gadow; A., Killinger; Lusvarghi, Luca; Sola, Antonella. - In: JOURNAL OF THERMAL SPRAY TECHNOLOGY. - ISSN 1059-9630. - STAMPA. - 21:(2012), pp. 275-287. [10.1007/s11666-011-9724-z]
N., Stiegler; Bellucci, Devis; Bolelli, Giovanni; Cannillo, Valeria; R., Gadow; A., Killinger; Lusvarghi, Luca; Sola, Antonella
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Utilizza questo identificativo per citare o creare un link a questo documento: https://hdl.handle.net/11380/736853
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