The thermal behaviour of single-crystals of the title compound has been investigated by means of thermal methods supported by optical microscopy. A complex change takes place on heating. After the loss of the two water molecules, leading to an amorphous phase, recrystallization takes place. This results in a solid (probably an anhydrous form) which reacts further, through partial liquefaction, to yield a red crystalline product whose structure has been characterized via X-ray powder spectra and electronic and IR spectroscopy
Thermal behaviour of [N(2-ammoniumethyl) piperazinium] pentachlorocuprate(II) dihydrate / J., Giusti; G. G. T., Guarini; Menabue, Ledi; Pellacani, Gian Carlo. - In: JOURNAL OF THERMAL ANALYSIS. - ISSN 0368-4466. - STAMPA. - 29:(1984), pp. 639-643. [10.1007/BF01913520]
Thermal behaviour of [N(2-ammoniumethyl) piperazinium] pentachlorocuprate(II) dihydrate
MENABUE, Ledi;PELLACANI, Gian Carlo
1984
Abstract
The thermal behaviour of single-crystals of the title compound has been investigated by means of thermal methods supported by optical microscopy. A complex change takes place on heating. After the loss of the two water molecules, leading to an amorphous phase, recrystallization takes place. This results in a solid (probably an anhydrous form) which reacts further, through partial liquefaction, to yield a red crystalline product whose structure has been characterized via X-ray powder spectra and electronic and IR spectroscopy
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