The present paper reports an optimized procedure for the efficient and fast HPLC-CSP separation of the enantiomeric pair of verapamil uusing a chiral column with alpha-acid glycoprotein as selector. The influence of temperature, pH, flow-rate and concentration of organic modifier on the chromatographic separations is shown.
Separation of chiral compounds with alpha-acid glycoprotein as selector / Gamberini, Gianfranco; Ferioli, Valeria; Rustichelli, Cecilia; Vezzalini, Francesca. - In: ATTI DELLA SOCIETÀ DEI NATURALISTI E MATEMATICI DI MODENA. - ISSN 0365-7027. - STAMPA. - 121:(1990), pp. 111-120.
Separation of chiral compounds with alpha-acid glycoprotein as selector
GAMBERINI, Gianfranco;FERIOLI, Valeria;RUSTICHELLI, Cecilia;VEZZALINI, Francesca
1990
Abstract
The present paper reports an optimized procedure for the efficient and fast HPLC-CSP separation of the enantiomeric pair of verapamil uusing a chiral column with alpha-acid glycoprotein as selector. The influence of temperature, pH, flow-rate and concentration of organic modifier on the chromatographic separations is shown.
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