Synthesis, Crystal and Molecular Structure, and Infrared Characterization of Two Amino Derivatives of 1,3,4–Thiadiazole

Antolini, Luciano; Cornia, Andrea; Fabretti Costantino, Antonio; Malavasi, Wanda

2-Amino-5-methyl-1,3,4-thiadiazole, 2-amino-5-methyl-3H-1,3,4-thiadiazolium bromide [(amtzH)(amtz)Br] and bis(2,5-diamino-3H-1,3,4-thiadiazolium) sulfate [(a2tzH)2SO4] were prepd. and characterized by x-ray structural anal. and IR spectroscopy. The crystals of (amtzH)(amtz)Br are monoclinic. Its asym. unit contains one protonated amtzH cation, one neutral amtz mol., and one bromide ion. The crystals of (a2tzH)2SO4 are monoclinic. The structure is built up of one crystallog. independent a2tzH cation and one half sulfate ion with crystallog. dictated twofold symmetry.

Synthesis, Crystal and Molecular Structure, and Infrared Characterization of Two Amino Derivatives of 1,3,4–Thiadiazole / Antolini, Luciano; Cornia, Andrea; FABRETTI COSTANTINO, Antonio; Malavasi, Wanda. - In: JOURNAL OF CRYSTALLOGRAPHIC AND SPECTROSCOPIC RESEARCH. - ISSN 0277-8068. - STAMPA. - 23(1993), pp. 967-971.

Data di pubblicazione:	1993
Titolo:	Synthesis, Crystal and Molecular Structure, and Infrared Characterization of Two Amino Derivatives of 1,3,4–Thiadiazole
Autore/i:	Antolini, Luciano; Cornia, Andrea; FABRETTI COSTANTINO, Antonio; Malavasi, Wanda
Autore/i UNIMORE:	ANTOLINI, Luciano CORNIA, Andrea FABRETTI COSTANTINO, Antonio MALAVASI, Wanda
Rivista:	JOURNAL OF CRYSTALLOGRAPHIC AND SPECTROSCOPIC RESEARCH
Volume:	23
Pagina iniziale:	967
Pagina finale:	971
Codice identificativo ISI:	WOS:A1993MP50000012
Codice identificativo Scopus:	2-s2.0-0001654088
Citazione:	Synthesis, Crystal and Molecular Structure, and Infrared Characterization of Two Amino Derivatives of 1,3,4–Thiadiazole / Antolini, Luciano; Cornia, Andrea; FABRETTI COSTANTINO, Antonio; Malavasi, Wanda. - In: JOURNAL OF CRYSTALLOGRAPHIC AND SPECTROSCOPIC RESEARCH. - ISSN 0277-8068. - STAMPA. - 23(1993), pp. 967-971.
Tipologia	Articolo su rivista

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