Polyetheretherketone (PEEK)-Al2O3 composite coatings have been successfully deposited on 316L stainlesssteel substrates by electrophoretic deposition (EPD) from ethanolic suspensions containing nanosize aluminaand micrometric PEEK particles. Uniform composite coatings containing between 20 and 70 wt.% of PEEKhave been obtained. An electrostatic interaction between the two kinds of particles has been confirmed byzeta potential and TEM analysis. The EPD yield increased with deposition time and difference of potentialapplied following a logarithmic trend. Reproducible PEEK-alumina coatings were deposited. A heat treatmentat 343 °C for 30 min with a heating rate 10 °C min−1 was needed to increase the adhesion substrate-coating.EPD can be considered a convenient low cost method to produce PEEK-Al2O3 composite films on metallicsubstrates. Scratch test analysis and hardness measurements showed that the deposited coatings were toorich in alumina and that a lower amount of alumina would be enough to satisfactorily increase themechanical properties. The corrosion resistance of the coatings in chlorine environment was tested. It wasshown that PEEK-alumina composite coatings performed better than pure PEEK films and exhibited asignificant increase in the pitting potential compared to uncoated stainless steel substrate.
Electrophoretic deposition of PEEK-nano alumina composite coatings on stainless steel / Ilaria, Corni; Nico, Neumann; Saa, Novak; Katja, König; Veronesi, Paolo; Qizhi, Chen; MARY P., Ryan; ALDO R., Boccaccini. - In: SURFACE & COATINGS TECHNOLOGY. - ISSN 0257-8972. - STAMPA. - 203:10-11(2009), pp. 1349-1359. [10.1016/j.surfcoat.2008.11.005]
Electrophoretic deposition of PEEK-nano alumina composite coatings on stainless steel
VERONESI, Paolo;
2009
Abstract
Polyetheretherketone (PEEK)-Al2O3 composite coatings have been successfully deposited on 316L stainlesssteel substrates by electrophoretic deposition (EPD) from ethanolic suspensions containing nanosize aluminaand micrometric PEEK particles. Uniform composite coatings containing between 20 and 70 wt.% of PEEKhave been obtained. An electrostatic interaction between the two kinds of particles has been confirmed byzeta potential and TEM analysis. The EPD yield increased with deposition time and difference of potentialapplied following a logarithmic trend. Reproducible PEEK-alumina coatings were deposited. A heat treatmentat 343 °C for 30 min with a heating rate 10 °C min−1 was needed to increase the adhesion substrate-coating.EPD can be considered a convenient low cost method to produce PEEK-Al2O3 composite films on metallicsubstrates. Scratch test analysis and hardness measurements showed that the deposited coatings were toorich in alumina and that a lower amount of alumina would be enough to satisfactorily increase themechanical properties. The corrosion resistance of the coatings in chlorine environment was tested. It wasshown that PEEK-alumina composite coatings performed better than pure PEEK films and exhibited asignificant increase in the pitting potential compared to uncoated stainless steel substrate.
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