Microwave assisted decomposition of germanium(IV) sulphide has been used to obtain, by sublimation in He current, amorphous particles of germanium(II) sulphide in the 0.1-3.0 microns range. The adopted technique is reported in details as well as the full physical-chemical characterisation of the product (XRD, TEM, Raman, MS and dielectric properties).
AMORPHOUS GERMANIUM (II) SULPHIDE PARTICLES OBTAINED BY MICROWAVE ASSISTED DECOMPOSITION OF GERMANIUM (IV) DISULFIDE / E., Bonometti; M., Castiglioni; P., MICHELIN LAUSAROT; Leonelli, Cristina; Bondioli, Federica; Pellacani, Gian Carlo; A. A., Barba. - In: MATERIALS RESEARCH INNOVATIONS. - ISSN 1432-8917. - STAMPA. - 10[2]:(2006), pp. 148-168.
AMORPHOUS GERMANIUM (II) SULPHIDE PARTICLES OBTAINED BY MICROWAVE ASSISTED DECOMPOSITION OF GERMANIUM (IV) DISULFIDE
LEONELLI, Cristina;BONDIOLI, Federica;PELLACANI, Gian Carlo;
2006
Abstract
Microwave assisted decomposition of germanium(IV) sulphide has been used to obtain, by sublimation in He current, amorphous particles of germanium(II) sulphide in the 0.1-3.0 microns range. The adopted technique is reported in details as well as the full physical-chemical characterisation of the product (XRD, TEM, Raman, MS and dielectric properties).
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