A range of characterization methods were used to measure size and distribution of sizes of the ZrO2 nanocrystals synthesized hydrothermally in a microwave heated high pressure reactor [1-4]. The aim of the work is to compare size readings of the same ceramics nanopowders as reported by different characterization methods. We describe briefly capabilities of TEM, XRD and BET characterization techniques, such as size vs. size distribution output, crystalline phase resolution, ability of error estimation of the size as well as dispersion of sizes readings (error bars: yes/no).
Grain size and grain size distibution of zro<>2<>:Pr ceramics nanopowders determined by different methods / Opalinska, A.; Pielaszek, R.; Lojkowski, W.; Leonelli, C.; Matysiak, H.; Wejrzanowski, T.; Kurzydlowski, K. J.. - 2:(2009), pp. 702-707. (Intervento presentato al convegno 11th International Conference and Exhibition of the European Ceramic Society 2009 tenutosi a Krakow, pol nel 2009).
Grain size and grain size distibution of zro<>2<>:Pr ceramics nanopowders determined by different methods
Leonelli C.;
2009
Abstract
A range of characterization methods were used to measure size and distribution of sizes of the ZrO2 nanocrystals synthesized hydrothermally in a microwave heated high pressure reactor [1-4]. The aim of the work is to compare size readings of the same ceramics nanopowders as reported by different characterization methods. We describe briefly capabilities of TEM, XRD and BET characterization techniques, such as size vs. size distribution output, crystalline phase resolution, ability of error estimation of the size as well as dispersion of sizes readings (error bars: yes/no).
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