Developing simple and effective chemistry able to convert industrial waste streams into valuable chemicals is a primary contributor to sustainable development. Working in the context of biodiesel production, we found that plain bisulfate on silica (SSANa, 3.0 mmol/g) proved to be an optimal catalyst to convert glycerol into solketal. With the assistance of a proper anhydrification technique, isolated yields of 96% were achieved working in mild conditions, on 100 g scale.
An expedient catalytic process to obtain solketal from biobased glycerol / Roncaglia, F.; Forti, L.; D'Anna, S.; Maletti, L.. - In: PROCESSES. - ISSN 2227-9717. - 9:1(2021), pp. 1-12. [10.3390/pr9010141]
An expedient catalytic process to obtain solketal from biobased glycerol
Roncaglia F.
;Forti L.;Maletti L.
2021
Abstract
Developing simple and effective chemistry able to convert industrial waste streams into valuable chemicals is a primary contributor to sustainable development. Working in the context of biodiesel production, we found that plain bisulfate on silica (SSANa, 3.0 mmol/g) proved to be an optimal catalyst to convert glycerol into solketal. With the assistance of a proper anhydrification technique, isolated yields of 96% were achieved working in mild conditions, on 100 g scale.
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