A methodology for the simultaneous detection of several heavy metals in water samples is described in detail. Targets were chemically prepared by preconcentration of the metals. Characteristics of the proton beam and X-ray detection are summarized. The concentration was obtained by using an internal standard in the range ppb-ppm. The method was tested by calibration with samples of known concentration. The subtraction of background and the data processing are discussed. The error in each concentration is evaluated.
CALIBRATION AND ERRORS IN THE DETECTION OF HEAVY METALS IN FRESH AND SEA WATER BY PIXE IN THE PPB-PPM RANGE / Aprilesi, Giancarlo; Cecchi, Rodolfo; Ghermandi, Grazia; Magnoni, Gaetano; Santangelo, Renato. - In: NUCLEAR INSTRUMENTS & METHODS IN PHYSICS RESEARCH. SECTION B, BEAM INTERACTIONS WITH MATERIALS AND ATOMS. - ISSN 0168-583X. - 231:1-3(1984), pp. 172-176. (Intervento presentato al convegno Part Induced X-Ray Emiss and its Anal Appl 3, Proc of the Int Conf, 3rd tenutosi a Heidelberg, W Ger, nel 1983).
CALIBRATION AND ERRORS IN THE DETECTION OF HEAVY METALS IN FRESH AND SEA WATER BY PIXE IN THE PPB-PPM RANGE
Aprilesi Giancarlo;Cecchi Rodolfo;Ghermandi Grazia;Santangelo Renato
1984
Abstract
A methodology for the simultaneous detection of several heavy metals in water samples is described in detail. Targets were chemically prepared by preconcentration of the metals. Characteristics of the proton beam and X-ray detection are summarized. The concentration was obtained by using an internal standard in the range ppb-ppm. The method was tested by calibration with samples of known concentration. The subtraction of background and the data processing are discussed. The error in each concentration is evaluated.Pubblicazioni consigliate
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