We report the isolation and characterization of bisadducts of fulleropyrrolidine derivatives. The compounds were characterized by means of a variety of spectroscopic techniques, including ESMS, UV-vis, 1H NMR, and 13C NMR. The whole series of bisadducts was separated for the first time in the case of the bispyrrolidines, and the determination of their structure was obtained by NMR spectroscopy with the help of HMQC and HMBC techniques.
Isolation and characterization of all eight bisadducts of fulleropyrrolidine derivatives / Kordatos, K.; Bosi, S.; Da Ros, T.; Zambon, Alfonso; Lucchini, V.; Prato, M.. - In: JOURNAL OF ORGANIC CHEMISTRY. - ISSN 0022-3263. - 66:8(2001), pp. 2802-2808. [10.1021/jo001708z]
Isolation and characterization of all eight bisadducts of fulleropyrrolidine derivatives
ZAMBON, Alfonso;
2001
Abstract
We report the isolation and characterization of bisadducts of fulleropyrrolidine derivatives. The compounds were characterized by means of a variety of spectroscopic techniques, including ESMS, UV-vis, 1H NMR, and 13C NMR. The whole series of bisadducts was separated for the first time in the case of the bispyrrolidines, and the determination of their structure was obtained by NMR spectroscopy with the help of HMQC and HMBC techniques.
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