Alpha-Chlorodimethylacetals are hydrolysed in a mixture of acetic acid and aq. HCI (3.5 M) to alpha-chloroaldehydes in excellent yields. On replacing HCI by HBr the same procedure is applied to alpha-bromodimethylacetals.
REGENERATION OF ALPHA-HALOALDEHYDES FROM ALPHA-HALODIMETHYLACETALS / Boni, M; Ghelfi, Franco; Pagnoni, Ugo Maria; Pinetti, Adriano. - In: SYNTHETIC COMMUNICATIONS. - ISSN 0039-7911. - STAMPA. - 23:(1993), pp. 1915-1921.
REGENERATION OF ALPHA-HALOALDEHYDES FROM ALPHA-HALODIMETHYLACETALS
GHELFI, Franco;PAGNONI, Ugo Maria;PINETTI, Adriano
1993
Abstract
Alpha-Chlorodimethylacetals are hydrolysed in a mixture of acetic acid and aq. HCI (3.5 M) to alpha-chloroaldehydes in excellent yields. On replacing HCI by HBr the same procedure is applied to alpha-bromodimethylacetals.
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