The synthesis and crystal and molecular structure of the title compound is reported. It belongs to the monoclinic space groupP21/a witha=29.3990 (20),b=7.1150 (6),c=8.3140 (9) Å, =98.060 (9)° andZ=4. The structure was refined to a finalR of 3.52% (R w %=3.82) for 2354 observed reflections. Vibrational spectra have been recorded and discussed.
Structural and spectral study of 7-chloro-3-hydroxy-1-methyl-5-phenyl-1,3-dihydro-2H-1,4-benzodiazepin-2-one (temazepam) mercury (II) dichloride / L., Antolini; C., Preti; G., Tosi; Zannini, Paolo. - In: JOURNAL OF CRYSTALLOGRAPHIC AND SPECTROSCOPIC RESEARCH. - ISSN 0277-8068. - STAMPA. - 16:(1986), pp. 115-124.
Structural and spectral study of 7-chloro-3-hydroxy-1-methyl-5-phenyl-1,3-dihydro-2H-1,4-benzodiazepin-2-one (temazepam) mercury (II) dichloride
ZANNINI, Paolo
1986
Abstract
The synthesis and crystal and molecular structure of the title compound is reported. It belongs to the monoclinic space groupP21/a witha=29.3990 (20),b=7.1150 (6),c=8.3140 (9) Å, =98.060 (9)° andZ=4. The structure was refined to a finalR of 3.52% (R w %=3.82) for 2354 observed reflections. Vibrational spectra have been recorded and discussed.Pubblicazioni consigliate
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