This paper reports results that show the effect of microwave absorption on the bulk crystallization of two glasses in the CaO-ZrO2SiO2 system. The glass samples were de vitrified using either microwave or conventional heating, to compare the results obtained from the two different techniques. Remarkably different crystallization paths were observed, depending mostly on the composition of the glass. This observation was especially true when microwave heating was used, where the dielectric losses observed in silicate glasses are related to the ZrO2 content. X-ray diffraction analysis was performed on the powdered samples, to determine the crystalline phases present. The microstructure and microanalysis results of these glass-ceramic compositions are presented and are related to the different ZrO2 contents.
Bulk crystallization of glasses belonging to the calcia-zirconia-silica system by microwave energy / Siligardi, Cristina; Mc, D'Arrigo; Leonelli, Cristina; Pellacani, Gian Carlo; Te, Cross. - In: JOURNAL OF THE AMERICAN CERAMIC SOCIETY. - ISSN 0002-7820. - STAMPA. - 83:4(2000), pp. 1001-1003. [10.1111/j.1151-2916.2000.tb01318.x]
Bulk crystallization of glasses belonging to the calcia-zirconia-silica system by microwave energy
SILIGARDI, Cristina;LEONELLI, Cristina;PELLACANI, Gian Carlo;
2000
Abstract
This paper reports results that show the effect of microwave absorption on the bulk crystallization of two glasses in the CaO-ZrO2SiO2 system. The glass samples were de vitrified using either microwave or conventional heating, to compare the results obtained from the two different techniques. Remarkably different crystallization paths were observed, depending mostly on the composition of the glass. This observation was especially true when microwave heating was used, where the dielectric losses observed in silicate glasses are related to the ZrO2 content. X-ray diffraction analysis was performed on the powdered samples, to determine the crystalline phases present. The microstructure and microanalysis results of these glass-ceramic compositions are presented and are related to the different ZrO2 contents.
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