[GRAPHICS] The (PhO)(3)P.CL2 reagent, prepared in situ by titrating a solution of triphenyl phosphite with chlorine, is used to convert N-monosubstituted amides into their corresponding amines. The reaction, if compared to other traditional methods, shows the advantage of very mild conditions and low temperature (-30 degreesC-->rt).
Low-temperature deacylation of N-monosubstituted amides / Spaggiari, Alberto; Blaszczak, L. C.; Prati, Fabio. - In: ORGANIC LETTERS. - ISSN 1523-7060. - STAMPA. - 6:22(2004), pp. 3885-3888. [10.1021/ol048852h]
Low-temperature deacylation of N-monosubstituted amides
SPAGGIARI, Alberto;PRATI, Fabio
2004
Abstract
[GRAPHICS] The (PhO)(3)P.CL2 reagent, prepared in situ by titrating a solution of triphenyl phosphite with chlorine, is used to convert N-monosubstituted amides into their corresponding amines. The reaction, if compared to other traditional methods, shows the advantage of very mild conditions and low temperature (-30 degreesC-->rt).
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