Balsamic vinegar of Modena (BVM) and traditional balsamic vinegar of Modena (TBVM) are highly appreciated typical Italian products. The quality control and authentication assurance of both these balsamic vinegars are very important topics. In the recent years, the interest to develop new and standardized analytical procedures, able to further enhance the quality and commercial value of these typical and unique products and to preserve them from possible sophistications and adulterations, is increased. In this work, 76 samples of both BVM and TBVM were analized by 1H NMR spectroscopy coupled with multivariate data analysis. The spectral data were analyzed by principal component analysis (PCA), general discriminant analysis (GDA) and classification tree analysis (CTA). The best and very promising model was obtained by a GDA which shows 98.6% of total variance explained by the first canonical function and a predictive capacity of 98.4% with a good separation between clusters. The signals of 5-HMF, -glucopyranose, malic acid, succinic and acetic acids and a signal at 3.3 ppm referred to the glucose and fructose region were found to be the most statistically significant variables.

Traditional balsamic vinegar and balsamic vinegar of Modena analyzed by nuclear magnetic resonance spectroscopy coupled with multivariate data analysis / Papotti, Giulia; Bertelli, Davide; Graziosi, Riccardo; Maietti, Annalisa; Tedeschi, Paola; Marchetti, Andrea; Plessi, Maria. - In: LEBENSMITTEL-WISSENSCHAFT + TECHNOLOGIE. - ISSN 0023-6438. - STAMPA. - 60:2(2015), pp. 1017-1024. [10.1016/j.lwt.2014.10.042]

Traditional balsamic vinegar and balsamic vinegar of Modena analyzed by nuclear magnetic resonance spectroscopy coupled with multivariate data analysis

PAPOTTI, GIULIA;BERTELLI, Davide;GRAZIOSI, RICCARDO;MARCHETTI, Andrea;PLESSI, Maria
2015

Abstract

Balsamic vinegar of Modena (BVM) and traditional balsamic vinegar of Modena (TBVM) are highly appreciated typical Italian products. The quality control and authentication assurance of both these balsamic vinegars are very important topics. In the recent years, the interest to develop new and standardized analytical procedures, able to further enhance the quality and commercial value of these typical and unique products and to preserve them from possible sophistications and adulterations, is increased. In this work, 76 samples of both BVM and TBVM were analized by 1H NMR spectroscopy coupled with multivariate data analysis. The spectral data were analyzed by principal component analysis (PCA), general discriminant analysis (GDA) and classification tree analysis (CTA). The best and very promising model was obtained by a GDA which shows 98.6% of total variance explained by the first canonical function and a predictive capacity of 98.4% with a good separation between clusters. The signals of 5-HMF, -glucopyranose, malic acid, succinic and acetic acids and a signal at 3.3 ppm referred to the glucose and fructose region were found to be the most statistically significant variables.
2015
23-ott-2014
60
2
1017
1024
Traditional balsamic vinegar and balsamic vinegar of Modena analyzed by nuclear magnetic resonance spectroscopy coupled with multivariate data analysis / Papotti, Giulia; Bertelli, Davide; Graziosi, Riccardo; Maietti, Annalisa; Tedeschi, Paola; Marchetti, Andrea; Plessi, Maria. - In: LEBENSMITTEL-WISSENSCHAFT + TECHNOLOGIE. - ISSN 0023-6438. - STAMPA. - 60:2(2015), pp. 1017-1024. [10.1016/j.lwt.2014.10.042]
Papotti, Giulia; Bertelli, Davide; Graziosi, Riccardo; Maietti, Annalisa; Tedeschi, Paola; Marchetti, Andrea; Plessi, Maria
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Utilizza questo identificativo per citare o creare un link a questo documento: https://hdl.handle.net/11380/1064052
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